Synthesis, Characterization and study properties of poly para chloro aniline and poly para chloroaniline\MnO2 nanocomposite
Abstract
In this work, by oxidative polymerization, we prepared poly para chloro aniline (P (p-ClAn)) and their composites with nano manganese dioxide (MnO2) in different percentages (13, 26, and52 %). It was characterization by the electronic scanning device, FT-IR infrared spectroscopy, H.N.M.R spectroscopy and differential scanning calorimetry, and also measured the electrical conductivity. By FT-IR and HNMR spectroscopy were confirmed of polymer structure, Also the material crystallinity was confirmed by characterization a differential scanning calorimetry (DSC). The electrical conductivity of the prepared polymer and their composites was also measured in different ratios and it was found that the conductivity decreases with the increase of the percentage of MnO2. The surface morphology analysis of P(p-ClAn) \MnO2 nanocomposite shows that polymer capped with inorganic material which is MnO2.
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